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Direct-ink writing of strong and biocompatible titanium scaffolds with bimodal interconnected porosity

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  • Additional Information
    • Contributors:
      Matériaux, ingénierie et science Villeurbanne (MATEIS); Université Claude Bernard Lyon 1 (UCBL); Université de Lyon-Université de Lyon-Institut National des Sciences Appliquées de Lyon (INSA Lyon); Université de Lyon-Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA)-Centre National de la Recherche Scientifique (CNRS)
    • Publication Information:
      HAL CCSD
      Elsevier
    • Publication Date:
      2021
    • Collection:
      Université de Lyon: HAL
    • Abstract:
      International audience ; Additive manufacturing of porous Ti6Al4V (Ti64) parts is promising for biomedical applications. In this study, Ti64 scaffolds with two scales of interconnected porosity networks were developed using a direct-ink writing process. Inks were made by dissolving a copolymer (Pluronic F-127) in water to obtain a hydrogel, which was then loaded with Ti64 particles. Both Pluronic F-127 amount in the hydrogel and solid loading influenced ink printability, as shown by rheological measurements and printing accuracy investigation. The best compromise was obtained for a 25 wt% Pluronic hydrogel loaded with 50 vol% of Ti64 particles. A partial sintering of 2 h at 1200 ∘ C led to interconnected micropores within strut, which was characterised by X-Ray computed tomography. Sintered scaffolds presented a compressive strength higher than bone, with a similar Young's modulus. According to their biocompatibility, final microstructure and mechanical properties, these scaffolds show a promising potential for load-bearing implants.
    • Relation:
      hal-03123169; https://hal.science/hal-03123169; https://hal.science/hal-03123169/document; https://hal.science/hal-03123169/file/Robocasting%20Ti%20Coffigniez%20AddMan%202021-HAL.pdf
    • Accession Number:
      10.1016/j.addma.2021.101859
    • Online Access:
      https://hal.science/hal-03123169
      https://hal.science/hal-03123169/document
      https://hal.science/hal-03123169/file/Robocasting%20Ti%20Coffigniez%20AddMan%202021-HAL.pdf
      https://doi.org/10.1016/j.addma.2021.101859
    • Rights:
      info:eu-repo/semantics/OpenAccess
    • Accession Number:
      edsbas.D3C2D29B